Ysi 3200 Manuale Utente

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YSI Model 3200
Conductance,
Resistance,
Salinity,
Total Dissolved Solids and
Temperature Instrument
Operations Manual
Vedere la pagina 0
1 2 3 4 5 6 ... 85 86

Sommario

Pagina 1 - YSI Model 3200

YSI Model 3200 Conductance, Resistance, Salinity, Total Dissolved Solids and Temperature Instrument Operations Manual

Pagina 2

Introduction Section 1 temperature sensor. All YSI 3200 series cells contain an internal temperature sensor; therefore, an external temperature prob

Pagina 3 - CONTENTS

SECTION 2 GETTING STARTED 2.1 UNPACKING When you unpack your new YSI Model 3200 for the first time, check the packing list to make sure you have re

Pagina 4

Getting Started Section 2 Units0.0000 uS K=1.000 25.0°C 11:33AM -10.00°C 1.91%/°C T CELL CELL SETUP DIAG RANGE OPERATION Soft key functionsI

Pagina 5 - SECTION 1 INTRODUCTION

Getting Started Section 2 3. Connect the Cell Plug the cell (YSI 3200 series) into the connector on the back of the instrument marked cell. NOTE:

Pagina 6 - FEATURES

Getting Started Section 2 5. Measurement After setting up the 3200 instrument and cell as described above, the following basic steps should be use

Pagina 7 - FRONT PANEL

SECTION 3 SYSTEM CONFIGURATION AND OPERATION 3.1 MENU The following section shows the software flow chart for the 3200. The two operating modes, Data

Pagina 8 - 1.953uS/cm

System Configuration and Operation Section 3 3.2 CELL CALIBRATION Before operating the 3200, or whenever you change cells, you must configure the 3

Pagina 9 - RS232 CONNECTION

System Configuration and Operation Section 3 [0] # Configuration number CONFIG [CONFIG 0] Title 0.0000uS offset [Single] Cell Cal [1.00

Pagina 10 - CE COMPLIANCE

System Configuration and Operation Section 3 Field Range / options Description %/°C comp val 0.0 - 10 Linear temperature compensation value. T

Pagina 11 - 0.0000 uS/cm

System Configuration and Operation Section 3 Entered standard solution CAL CELL K [961.00] uS/cm Conductivity 1.024 measured K 23.0°C

Pagina 13 - 4. Configure the 3200

System Configuration and Operation Section 3 3.150 uS/cm Km=1.124 25.0°C 11:33AM 24.38°C 1.50%/°C T CELL CELL SETUP DIAG RANGE OPERATION Curr

Pagina 14 - 5. Measurement

System Configuration and Operation Section 3 3. Measure a linear temperature compensation factor. 4. Measure a non-linear temperature compensatio

Pagina 15 - 3.1 MENU

System Configuration and Operation Section 3 4. Place the cell (and temperature probe, if used) in the solution at the first desired temperature p

Pagina 16 - 3.2 CELL CALIBRATION

System Configuration and Operation Section 3 Send From the Cell Temp menu, the [SEND] soft key may be used to send the current temperature compensa

Pagina 17

System Configuration and Operation Section 3 684 mg/L TDS 0.4 ppt SAL 1.91%/°C T CELL ENTER TO CHANGE UNITS SIZE NEXT LIGHT DARK MEAS

Pagina 18 - Single Point

System Configuration and Operation Section 3 CONTRAST The display contrast is adjusted from the Setup Display menu. 13.15 uS/cm K=0.100 25.0°C

Pagina 19 - Multi Point

System Configuration and Operation Section 3 1. From Operation mode, press the [SETUP] soft key, then, press [SYSTEM] to enter the Setup

Pagina 20 - 3.150 uS/cm

System Configuration and Operation Section 3 Since the cursor is already in the Key beep field, press [UP] or [DOWN] to change the status of the be

Pagina 21

System Configuration and Operation Section 3 13.2uS K=0.100 25.0°C 11:34AM 24.38°C 1.50%/°C T CELL CURRENT RANGE [9.50 - 99.99uS] CELL SE

Pagina 22

System Configuration and Operation Section 3 1017 uS/cm 10.3mS OPERATION 984.6 Ωcm 97.077 Ω K=0.098 25.0°C 691 mg/L TDS 0.5 ppt SAL 1.91%

Pagina 23 - 13.15uS/cm

CONTENTS 1. Introduction...

Pagina 24 - MEASUREMENT UNITS

System Configuration and Operation Section 3 YSI Incorporated Model 3200 26

Pagina 25 - 13.15 uS/cm

SECTION 4 DATA STORAGE AND RETRIEVAL From Operation mode, press the [MENU] key to enter Data mode. Data mode is used to store, review or delete read

Pagina 26

Data Storage and Retrieval Section 4 If you wish to store a record at a location other than the current one, use the [UP], [DOWN] and [DIGIT] soft

Pagina 27 - 13.15uS

Data Storage and Retrieval Section 4 RECALL From the Review menu, press the [RECALL] soft key to enter Recall mode and display the following menu.

Pagina 28 - 9.999uS

Data Storage and Retrieval Section 4 NOTE: It is not necessary to clear records before new data can be stored. The new data will overwrite the prev

Pagina 29 - 3.6 MAKING MEASUREMENTS

Data Storage and Retrieval Section 4 4.3 SEND While in the Data menu, the [SEND] soft key is used to send the current live display readings to a co

Pagina 30

Data Storage and Retrieval Section 4 The baud rate range is 1200 to 19200. After you have selected the parameters, press [MODE] once, to return to

Pagina 31 - 31.15 uS/cm

Data Storage and Retrieval Section 4 Comma Delimited Format, send (recalled data) 0 ,3/20/97, 5:37:17PM, 1234uS/cm ,23.45C ,K=0.09,1.91%/C, 9999uS

Pagina 32 - 3.152 uS/cm

Data Storage and Retrieval Section 4 To change the S interval, press the [NEXT] soft key to select the S interval field. Then, use the [UP], [DOWN]

Pagina 33

SECTION 5 DIAGNOSTICS The YSI 3200 has a diagnostic mode that is used to test RS232 communications and the internal beeper. From the Operation menu,

Pagina 34 - CLEAR ALL

7. Troubleshooting...

Pagina 35

Diagnostics Section 5 YSI Incorporated Model 3200 36

Pagina 36

SECTION 6 MAINTENANCE 6.1 CELL CLEANING AND STORAGE The single most important requirement for accurate and reproducible results in conductivity mea

Pagina 37 - DATA LOGGING

Maintenance Section 6 2. Use the [UP], [DOWN] and [DIGIT] soft keys to enter the platinization time required in minutes. Six minutes is usually suf

Pagina 38

SECTION 7 TROUBLESHOOTING 7.1 ERROR MESSAGES The instrument performs a Power On Self Test each time it is turned on. The following error messages ar

Pagina 39 - SECTION 5 DIAGNOSTICS

Troubleshooting Section 7 YSI Incorporated Model 3200 40

Pagina 40 - Diagnostics Section 5

SECTION 8 PRINCIPLES OF OPERATION 8.1 RATIOMETRIC CONDUCTIVITY The basic concept of microprocessor based ratiometric conductivity measurement is to

Pagina 41 - SECTION 6 MAINTENANCE

Principles of Operation Section 8 Looking at our electrodes as sides of a cube, it becomes apparent that the conductance changes as the geometry o

Pagina 42

Principles of Operation Section 8 or less have larger electrodes that are closely-spaced. CHOOSING A CONDUCTIVITY CELL Decide which cell will be

Pagina 43 - SECTION 7 TROUBLESHOOTING

Principles of Operation Section 8 3252 3253 3254 3255 3256 YSI Incorporated Model 3200 44

Pagina 44 - Troubleshooting Section 7

Principles of Operation Section 8 CELL CONSTANT CALCULATION YSI 3200 and 3400 Series conductivity cells are calibrated to ± 1% of nominal by mean

Pagina 45 - CONDUCTIVITY FUNDAMENTALS

SECTION 1 INTRODUCTION The Model 3200 is a microprocessor based; menu-driven instrument designed to perform laboratory measurement of conductivity,

Pagina 46 - = k K

Principles of Operation Section 8 CONDUCTIVITY LAW SOLUTION INSTRUMENT CELL CONDUCTIVITY CONDUCTANCE CONSTANT S/cm or mho/cm = S or mho ×

Pagina 47 - CHOOSING A CONDUCTIVITY CELL

Principles of Operation Section 8 GENERAL CONDUCTIVITY MEASUREMENT PRECAUTIONS After selecting the proper cell, observe the following precaution

Pagina 48 - 3252 3253 3254 3255 3256

Principles of Operation Section 8 temperature coefficient. In extreme cases, the temperature coefficient may have a value as high as 7%/°C. Each c

Pagina 49 - CELL CONSTANT CALCULATION

Principles of Operation Section 8 SMALL SAMPLE MEASUREMENTS It is not always possible to immerse the conductivity cell in a solution for measureme

Pagina 50 - Error Sources

Principles of Operation Section 8 8.3 SALINITY Salinity is determined automatically from the Model 3200 conductivity and temperature readings acco

Pagina 51 - TEMPERATURE CORRECTION

Principles of Operation Section 8 ELECTRICAL-NOISE ERRORS Electrical noise can be a problem in any measurement range, but will contribute the most

Pagina 52 - 1 + (T - 25)

Principles of Operation Section 8 YSI Incorporated Model 3200 52

Pagina 53 - SMALL SAMPLE MEASUREMENTS

SECTION 9 WARRANTY AND REPAIR YSI Model 3200 Instruments are warranted for two years from date of purchase by the end user against defects in materi

Pagina 54

Warranty and Repair Section 9 AUTHORIZED U.S. SERVICE CENTERS FOR THE NEAREST AUTHORIZED SERVICE CENTER, CONTACT: YSI Technical Support • 1725 Bra

Pagina 55 - CONTACT RESISTANCE

Warranty and Repair Section 9 YSI Incorporated Model 3200 55

Pagina 56

Introduction Section 1 1.2 USER FEATURES • Audio feedback • Soft key/menu system • Real time clock • Auto linear temperature compensation calibr

Pagina 57

Warranty and Repair Section 9 CLEANING INSTRUCTIONS NOTE: Before they can be serviced, equipment exposed to biological, radioactive, or toxic mater

Pagina 58

Warranty and Repair Section 9 PACKING INSTRUCTIONS 1. Clean and decontaminate items to insure the safety of the handler. 2. Complete and include

Pagina 59

Warranty and Repair Section 9 9.1 SOFTWARE UPGRADE PROCEDURE If necessary, the YSI Model 3200’s software can be upgraded using a computer with a s

Pagina 60 - CLEANING INSTRUCTIONS

Warranty and Repair Section 9 9.2 DISASSEMBLY/ASSEMBLY PROCEDURES Place the instrument face down on a padded surface for all procedures below. Case

Pagina 61 - PACKING INSTRUCTIONS

Warranty and Repair Section 9 9.3 TEST AND VERIFICATION PROCEDURE Connect the YSI Model 3200 as shown in the Test and Verification Figure and foll

Pagina 62

Warranty and Repair Section 9 Temperature Verification Temperature Cell Connector Pin 1 & 2 Input Resistance ** EX. TEMP Connector Input Resis

Pagina 63 - Case Re-assembly

Warranty and Repair Section 9 Test and Verification Figure 3200’s 7-Pin Mini DIN Cell Connector Cell Thermistor 10K Ω@ 25 oC Conductivity Cell Cab

Pagina 64

SECTION 10 ACCESSORIES AND REPLACEMENT PARTS YSI Item # Description Comments 3208 Power Supply, 115 VAC 3209 Power Supply, 240 VAC 003213 Ov

Pagina 65

Accessories and Replacement Parts Section 10 10.1 YSI CONDUCTIVITY CELLS YSI 3200 series conductivity cells have a built in temperature sensor for

Pagina 66

Accessories and Replacement Parts Section 10 10.2 STANDARD CALIBRATOR SOLUTIONS YSI manufactures NIST-traceable conductivity calibrator solutions

Pagina 67

Introduction Section 1 1.3 CONTROLS FRONT PANEL The front panel of the instrument contains the display and keypad as shown below. OPERATION3200

Pagina 68 - 10.1 YSI CONDUCTIVITY CELLS

Accessories and Replacement Parts Section 10 YSI, Incorporated Model 3200 66

Pagina 69

APPENDIX A - SPECIFICATIONS Modes Conductivity Conductance Resistivity Resistance Salinity TDS Temperature

Pagina 70

Specifications Appendix A Temperature Compensation Method Linear, nonlinear Ref. temp., °C 0 - 100 Temp. Coef. 0 - 10%/°C, nonlinear

Pagina 71 - APPENDIX A - SPECIFICATIONS

APPENDIX B REQUIRED NOTICE This equipment generates and uses radio frequency energy and if not installed and used properly, may cause interference

Pagina 72 - Specifications Appendix A

Required Notice Appendix B YSI, Incorporated Model 3200 70

Pagina 73 - APPENDIX B REQUIRED NOTICE

APPENDIX C - RS232 CONNECTIONS Serial Printer Connection To connect to a serial printer, use a 9-pin male to 25 pin male cable. 3200: 9 pin d-sub (m

Pagina 74

RS232 Connections Appendix C YSI, Incorporated Model 3200 72

Pagina 75 - Serial Computer Connection

APPENDIX D TEMPERATURE CORRECTION DATA FOR TYPICAL SOLUTIONS A. Potassium Chloride** (KCl) Concentration: 1 mole/liter Concentratio

Pagina 76

Temperature Correction Data for Typical Solutions Appendix D B. Sodium Chloride* (NaCl) Saturated solutions at all temperatures Concentration: 0

Pagina 77 - TYPICAL SOLUTIONS

Temperature Correction Data for Typical Solutions Appendix D C. Lithium Chloride* (LiCl) Concentration: 1 mole/liter Concentration: 1 x 10-1 mol

Pagina 78 - (NaCl)

Introduction Section 1 The 3200 has two main operating modes, Data and Operation. The current mode is displayed in the dark bar at the top right cor

Pagina 79

Temperature Correction Data for Typical Solutions Appendix D E. Ammonium Chloride* (NH4Cl) Concentration: 1 mole/liter Concentration: 1 x 10-1 m

Pagina 80 - E. Ammonium Chloride

APPENDIX E - CONVERSION FACTORS TO CONVERT FROM TO EQUATION mhos Siemens Multiply by 1 mhos ohms 1/mho ohms mhos 1/ohm Feet Meters Multiply by

Pagina 81

Conversion Factors Appendix E YSI, Incorporated Model 3200 78

Pagina 82

APPENDIX F - GLOSSARY OF TERMS ampere (A) - SI unit of electric current; one coulomb per second. amplitude - The maximum deviation of an alternating

Pagina 83

Glossary of Terms Appendix F OIML - Organisation Internationale de Métrologie Légale is a treaty organization for the harmonization of practical ap

Pagina 84

Glossary of Terms Appendix F YSI Incorporated Model 3200 81

Pagina 85

1700/1725 Brannum Lane Yellow Springs, Ohio 45387 USA (800) 765-4974 • (937) 767-7241 FAX (937) 767-9353 Email:

Pagina 86

Introduction Section 1 REAR PANEL The rear panel contains the connections for the power supply, cell, external temperature probe and RS232 serial po

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